Articles

KUCHMA P.O., KUSHNIR A.G., ZEMCOVA O.V., BARANOV Yu.S. COMPLEX CONTROL MULTIRESIDUAL AMOUNTS OF PESTICIDES AND PAHS IN SOILS FOR VARIOUS PURPOSES

2016 – Zurnal Hromatografichnogo Tovarystva – V. XVI. – N 1-4. – P. 31-35

UDC 614.3:632.95:63-027.3:339.564

DOI: 10.15407 / zht2016.59.031

KUCHMA P.O., KUSHNIR A.G., ZEMCOVA O.V., BARANOV Yu.S. 

Ukrainian laboratory of quality and safety of agricultural products, Kyiv-Svyatoshinsky district, s.m.t. Chabany

COMPLEX CONTROL MULTIRESIDUAL AMOUNTS OF PESTICIDES AND PAHS IN SOILS FOR VARIOUS PURPOSES - article

In ULQSAP there was modified method of measuring pesticide residues in soil, based on the method of QuEChERS sample preparation, GC-MS and HPLC-MS-MS. The method meets the international metrological requirements under SANCO/12571/2013. The method was used for the control of soil contamination by agricultural land and soil zones of ecological disasters (the plant "Radical", dump chemical waste Kalush chemical plant, warehouse storage of obsolete pesticides, depot near Vasylkov). The method allows to determine not only pesticide residues, but also some PCBs and PAHs on MRL.

Key words: soil, pesticides, chromatography, mass spectrometry, ecological disaster, agriculture

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